Solution State

1. Please check the solubility of your samples before submitting samples for recording solution state NMR
2. Mention the deuterated solvent to be used for recording the NMR spectrum
3. Deuterated solvents available at our centre are CDCl₃, DMSO-D₆, D₂O,CD₃OD, CD₃COCD₃
4. The user has to provide the other deuterated solvents
5. Clearly mention the nucleus to be studied(¹H, ¹³C, ²⁹Si, ³¹P ,¹¹B etc) and the type of measurement(1D, DEPT, 2D,etc)
6. If you need, 2D measurement, clearly mention the type of measurement(COSY, DQFCOSY, NOESY, ROESY, HSQC, HMBC etc)
7. For Variable Temperature(VT) measurement, please mention the temperature range. Check the BP/MP of the solvent before selecting the temperature for VT experiments
8. If you are submitting your samples in NMR tubes, use only good quality NMR tubes(Wilmad, Norell, Sigma-Aldrich etc)

Sample Requirements

¹H: 5 -10 mg
¹³C, 2D etc: 20-30 mg